No. | sample | Step No., solid educts and solvent | Temp. (˚C) | time (h) | Products* (Wt %) |
13 | FR1-A | 1. FR 1 (2 g), NaOH (20 ml, 8 M) 2. Slurry 1+ H2O (30 ml) +NaAlO2 (2g)) + 20 ml H2O | 60 80 | 3 22 | Alkaline FR 1-slurry NaA |
14 | FR1-X | 1. FR 1 (2g), NaOH (20 ml, 8 M) 2. Slurry 1+ H2O (30 ml) +NaAlO2 (1.2 g) ) + 20 ml H2O | 60 90 | 3 16 | Alkaline FR 1-slurry NaX + INT-1 |
15 | FR2-A | 1. FR 2 (2g), NaOH (20 ml, 8 M) 2. Slurry 1+ H2O (20 ml) +NaAlO2 (1.6 g) + 10 ml H2O | 60 90 | 3 16 | Alkaline FR 2-slurry LTA NaA + NaX |
16 | FR2-X | 1. FR 2 (2g), NaOH (20 ml, 8 M) 2. Slurry 1+ H2O (30 ml) + NaAlO2 (0.5 g) + 20 ml H2O | 60 80 | 3 22 | Alkaline FR 2-slurry NaX |